Ag(2-chlorophenol)

Base Information

• Chemical Name: Ag(2-chlorophenol)
• CAS No.: 1010069-49-4
• Molecular Formula: Ag*C₆H₄ClO
• Molecular Weight: 235.418

Synonyms:

Chemical Property of Ag(2-chlorophenol)

Chemical Property:

Purity/Quality:

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Technology Process of Ag(2-chlorophenol)

There total 1 articles about Ag(2-chlorophenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

2-monochlorophenol (95-57-8) + silver nitrate → Ag(2-chlorophenol) (1010069-49-4)

Guidance literature:

With (C₂H₅)3N; In ethanol; acetonitrile; standard Schlenk techniques under N2; 2-chlorophenol dissolved in EtOH, Et3N added, mixture dropwise added to AgNO3 in EtOH/CH3CN at 0°C,stirred for 2 h at 0°C; collected, washed with EtOH and petroleum ether, dried in vac., elem. anal.;

DOI:10.1016/j.ica.2010.05.049

Reference yield: 99.0%

dichloromethane (75-09-2) + tributylphosphine (998-40-3) + Ag(2-chlorophenol) (1010069-49-4) → (tri-n-butylphosphine)2Ag(2-chlorophenol)*0.67CH2Cl2

Guidance literature:

In dichloromethane; standard Schlenk techniques under N2; nBu3P added to Ag-compd. (molar ratio 2:1) in CH2Cl2 at 25°C, stirred for 2 h at 25°C; filtered through a pad of Celite, all volatilies removed in vac., elem. anal.;

DOI:10.1016/j.ica.2010.05.049

Reference yield: 68.0%

tributylphosphine (998-40-3) + Ag(2-chlorophenol) (1010069-49-4) → (tri-n-butylphosphine)Ag(2-chlorophenol)

Guidance literature:

In dichloromethane; standard Schlenk techniques under N2; nBu3P added to Ag-compd. in CH2Cl2at 25°C, stirred for 2 h at 25°C; filtered, all volatilies removed in vac., elem. anal.;

DOI:10.1016/j.ica.2010.05.049

upstream raw materials:

2-monochlorophenol

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