2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

Base Information

Chemical Name:2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)
CAS No.:1337882-79-7
Molecular Formula:C₁₄H₁₀BrF₂N
Molecular Weight:310.141
Hs Code.:

2,6-F<sub>2</sub>C<sub>6</sub>H<sub>3</sub>CH=NCH<sub>2</sub>(2-BrC<sub>6</sub>H<sub>4</sub>)

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Chemical Property of 2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

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Technology Process of 2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

There total 1 articles about 2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.4%

: 437-81-0
2,6-difluorobenzaldehyde

: 5465-63-4
2-bromobenzylamine hydrochloride

: 1337882-79-7
2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

Guidance literature:: 2-bromobenzylamine hydrochloride; With potassium hydroxide; In water;

2,6-difluorobenzaldehyde; In ethanol; for 2h; Reflux;
DOI:10.1039/c1dt10664c

Reference yield: 39.0%

: 64827-19-6
bis[di(p-tolyl)(μ-diethyl sulfide)platinum(II)]

: 75-09-2
dichloromethane

: 1337882-79-7
2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

: 603-35-0
triphenylphosphine

: [PtBr(C₆H₃(4-CH₃C₆H₄)CH₂N=CH(2,6-C₆H₃F₂))PPh₃]*CH₂Cl₂

Guidance literature:: In benzene; byproducts: Pt; Pt complex and imine in benzene were heated under reflux for 4 h, solvent was removed in vacuo, soln. PPh3 in acetone was added, stirred for 2 hat room temp.; soln. was filtered and evapd., recrystn. from CH2Cl2-MeOH; elem. anal.;
DOI:10.1039/c1dt10664c

Reference yield:

: 64827-19-6
bis[di(p-tolyl)(μ-diethyl sulfide)platinum(II)]

: 1337882-79-7
2,6-F₂C₆H₃CH=NCH₂(2-BrC₆H₄)

: 1337882-83-3
[PtBr(C₆H₃(4-CH₃C₆H₄)CH₂N=CH(2,6-C₆H₃F₂))SEt₂]

Guidance literature:: In toluene; Pt complex and imine in toluene were heated under reflux for 4 h; soln. was filtered and evapd.;
DOI:10.1039/c1dt10664c