2,3-Dimethoxyphenol acetate

Base Information

• Chemical Name: 2,3-Dimethoxyphenol acetate
• CAS No.: 27257-08-5
• Molecular Formula: C₁₀H₁₂O₄
• Molecular Weight: 196.203
• Mol file: 27257-08-5.mol

Synonyms:

Chemical Property of 2,3-Dimethoxyphenol acetate

Chemical Property:

• Boiling Point: 246.2±25.0 °C(Predicted)
• Density: 1.120±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-Dimethoxyphenol acetate

There total 4 articles about 2,3-Dimethoxyphenol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dimethoxybenzene (91-16-7) + [bis(acetoxy)iodo]benzene (3240-34-4) → 3,4-dimethoxyphenyl acetate (7203-46-5) + 2,3-dimethoxyphenyl acetate (27257-08-5)

Guidance literature:

With palladium diacetate; In acetic anhydride; acetic acid; at 100 ℃; Reagent/catalyst; Overall yield = 35 %Chromat.;

DOI:10.1021/ol4024248

Reference yield:

1,2-dimethoxybenzene (91-16-7) + tetraethylammonium acetate (1185-59-7) → 2,3-dimethoxyphenyl acetate (27257-08-5)

Guidance literature:

With zinc(II) chloride; In acetonitrile; Electrolysis;

DOI:10.1016/j.mencom.2008.07.008

Reference yield:

2,3-dimethoxyphenol (5150-42-5) + acetyl chloride (75-36-5) → 2,3-dimethoxyphenyl acetate (27257-08-5)

Guidance literature:

upstream raw materials:

2,3-dimethoxyphenol

acetyl chloride

1,2-dimethoxybenzene

tetraethylammonium acetate

Downstream raw materials:

2'-hydroxy-3',4'-dimethoxyacetophenone

Refernces

• 1、 Burasov, Alexander V.,Petrosyan, Vladimir A.. "Electrophilic components in the electrochemical acetoxylation of substituted arenes". . p. 196 - 197. Retrieved 2008/12/22.