(ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄

Base Information

Chemical Name:(ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄
CAS No.:373603-16-8
Molecular Formula:C₁₁H₃₆ClN₄O₉P₃Re*C₂₄H₂₀B
Molecular Weight:1002.24
Hs Code.:

(ReCl(MeN<sub>2</sub>)(MeNHNH<sub>2</sub>)(P(OMe)3)3)BPh<sub>4</sub>

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Chemical Property of (ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄

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Technology Process of (ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄

There total 1 articles about (ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 87863-04-5,608133-96-6
ReOCl3(triphenylarsine)2

: 143-66-8
sodium tetraphenyl borate

: 60-34-4
methylhydrazine

: 121-45-9
phosphorous acid trimethyl ester

: 373603-16-8
(ReCl(MeN₂)(MeNHNH₂)(P(OMe)3)3)BPh₄

Guidance literature:: With NEt₃; In tetrahydrofuran; methanol; excess phospite was added to soln. ReOCl3(AsPh3)2 in THF and stirred for1 h, excess NEt3 and MeNHNH2 in MeOH were added and stirred for 3 h, so lvent was removed, residue was treated with MeOH soln. NaBPh4; ppt. was filtered, and crystd. from CH2Cl2 and EtOH; elem. anal.;
DOI:10.1021/ic0104508