(bis(diphenylarsino)methane-AsAs')dibromoplatinum

Base Information

Chemical Name:(bis(diphenylarsino)methane-AsAs')dibromoplatinum
CAS No.:106583-87-3
Molecular Formula:C₂₅H₂₂As₂Br₂Pt
Molecular Weight:827.181
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (bis(diphenylarsino)methane-AsAs')dibromoplatinum

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Technology Process of (bis(diphenylarsino)methane-AsAs')dibromoplatinum

There total 2 articles about (bis(diphenylarsino)methane-AsAs')dibromoplatinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 98169-71-2
(bis(diphenylarsino)methane-AsAs')dichloroplatinum

: 7550-35-8
lithium bromide

: 106583-87-3
(bis(diphenylarsino)methane-AsAs')dibromoplatinum

Guidance literature:: In acetone; PtCl2(CH2(AsPh2)2) suspended in acetone, excess LiBr added, boiled for 15 min; evapd. in vac., triturated with MeOH, solid filtered off, dried in vac.; elem. anal.;
DOI:10.1039/DT9870000151

Reference yield:

: 21892-63-7
bis(diphenylarsino)methane

: 106583-87-3
(bis(diphenylarsino)methane-AsAs')dibromoplatinum

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: acetone

In acetone; acetonitrile;
DOI:10.1039/DT9870000151

Reference yield: 89.0%

: 106583-87-3
(bis(diphenylarsino)methane-AsAs')dibromoplatinum

: 21892-63-7
bis(diphenylarsino)methane

: trans-bis(bis(diphenylarsino)methane-As)dibromoplatinum * 0.2 dichloromethane

Guidance literature:: With CH₂Cl₂; In dichloromethane; suspn. of PtBr2(CH2(AsPh2)2) in CH2Cl2 treated with 1 equiv. of CH2(AsPh2)2, mixt. boiled for 5 min; evapd. in vac., triturated with Et2O, solid filtered off, washed with Et2O, dried in vac.; elem. anal.;
DOI:10.1039/DT9870000151