3,3-dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

Base Information

• Chemical Name: 3,3-dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one
• CAS No.: 879132-47-5
• Molecular Formula: C₁₃H₁₈Br₂N₂O₂Si
• Molecular Weight: 422.192
• Hs Code.: 2933990090
• Mol file: 879132-47-5.mol

Synonyms:3,3-dibroMo-1-((2-(triMethylsilyl)ethoxy)Methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one;2H-Pyrrolo[2,3-b]pyridin-2-one, 3,3-dibroMo-1,3-dihydro-1-[[2-(triMethylsilyl)ethoxy]Methyl]-

Chemical Property of 3,3-dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

Chemical Property:

• Boiling Point: 456.9±45.0 °C(Predicted)
• PKA: 0.24±0.40(Predicted)
• PSA: 42.43000
• Density: 1.551±0.06 g/cm3(Predicted)
• LogP: 3.74810
• Storage Temp.: 2-8°C

Purity/Quality:

≥95% ^*data from raw suppliers

3,3-Dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

There total 4 articles about 3,3-dibromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridine (879132-46-4) → 3,3-dibromo-1-{[2-(trimethylsilyl)ethoxy]methyl}-1,3-dihydro-2H-pyrrolo[2.3-b]pyridin-2-one (879132-47-5)

Guidance literature:

With pyridinium hydrobromide perbromide; In 1,4-dioxane;

Reference yield:

7-Azaindole (271-63-6) → 3,3-dibromo-1-{[2-(trimethylsilyl)ethoxy]methyl}-1,3-dihydro-2H-pyrrolo[2.3-b]pyridin-2-one (879132-47-5)

Guidance literature:

With pyridinium hydrobromide perbromide; In 1,4-dioxane; at 20 ℃; for 1.5h;

Reference yield:

C13H18Br4N2OSi → 3,3-dibromo-1-{[2-(trimethylsilyl)ethoxy]methyl}-1,3-dihydro-2H-pyrrolo[2.3-b]pyridin-2-one (879132-47-5)

Guidance literature:

With water;

upstream raw materials:

1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridine

7-Azaindole

(2-trimethylethylsilylethoxy)methyl chloride

Downstream raw materials:

1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

spiro[piperidine-4,3'-pyrrolo[2,3-b]pyridin]-2'(1'H)-one

spiro[cyclopropane-1,3'-pyrrolo[2,3-b]pyridin]-2'(1'H)-one

5-nitro-1‘-((2-(trimethylsilyl)ethoxy)methyl)-1,3-dihydrospiro[indene-2,3’-pyrrolo[2,3-b]pyridin]-2’(1’H)-one

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