Methyl 3-((S)-1-phenylethylaMino)butanoate

Base Information

• Chemical Name: Methyl 3-((S)-1-phenylethylaMino)butanoate
• CAS No.: 1156032-60-8
• Molecular Formula: C13H19NO2
• Molecular Weight: 221.3
• Mol file: 1156032-60-8.mol

Synonyms:Methyl 3-((S)-1-phenylethylaMino)butanoate;Butanoic acid, 3-[[(1S)-1-phenylethyl]amino]-, methyl ester

Chemical Property of Methyl 3-((S)-1-phenylethylaMino)butanoate

Chemical Property:

• PSA: 38.33000
• LogP: 2.67970

Purity/Quality:

≥95% ^*data from raw suppliers

methyl3-((S)-1-phenylethylamino)butanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-((S)-1-phenylethylaMino)butanoate

There total 25 articles about Methyl 3-((S)-1-phenylethylaMino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + tert-butyl (3S,αS)-3-[N-(α-methylbenzyl)amino]butanoate (164660-11-1) → (3S,1'S)-3-<(1'-phenylethyl)amino>butanoic acid methyl ester (103123-51-9,1156032-60-8)

Guidance literature:

With hydrogenchloride;

DOI:10.1039/c39950001109

Reference yield: 91.0%

methyl (3R,αR,α'R)-3-(N,N-bis(α-methylbenzyl)amino)butanoate (134431-02-0) → (R)-methyl 3-[(R)-1-phenylethylamino]butanoate (1156032-60-8)

Guidance literature:

With hydrogen; palladium dihydroxide; In methanol; under 760 Torr;

DOI:10.1016/S0040-4039(98)01193-9

Reference yield: 90.0%

methyl (3R,αR)-3-(N-benzyl-N-α-methylbenzylamino)butanoate (134430-97-0) → (R)-methyl 3-[(R)-1-phenylethylamino]butanoate (1156032-60-8)

Guidance literature:

With hydrogen; palladium dihydroxide; In methanol; under 760 Torr;

DOI:10.1016/S0040-4039(98)01193-9

upstream raw materials:

crotonic acid methyl ester

rac-methylbenzylamine

(S)-1-phenyl-ethylamine

methyl crotonate

Downstream raw materials:

methyl 3-(R)-[N-(tert-butoxycarbonyl)amino]-propanoate

3-(4-chlorophenyl)-6-(S)-methyl-1-[(S)-1-phenylethyl]-2-thioxotetrahydropyrimidin-4(1H)-one

3-(3-chloro-4-fluorophenyl)-6-(S)-methyl-1-[(S)-1-phenylethyl]-2-thioxotetrahydropyrimidin-4(1H)-one

3-(3-chloro-4-cyanophenyl)-6-(S)-methyl-1-[(S)-1-phenylethyl]-2-thioxotetrahydropyrimidin-4(1H)-one

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