Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, formate

Base Information

• Chemical Name: Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, formate
• CAS No.: 100101-30-2
• Molecular Formula: C₁₁H₁₈O₂
• Molecular Weight: 182.263
• Mol file: 100101-30-2.mol

Synonyms:

Chemical Property of Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, formate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, formate

There total 16 articles about Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

Dimethyl-(1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yloxymethylene)-ammonium; chloride (100033-37-2) → isobornyl formate (74219-20-8,100101-30-2)

Guidance literature:

With sulfuric acid;

DOI:10.1055/s-1985-31228

Reference yield:

formic acid (64-18-6) → isobornyl formate (74219-20-8,100101-30-2)

Guidance literature:

With sulfuric acid; at 30 ℃; formic acid dl-isobornyl ester;

Reference yield:

1,7,7-trimethyl bicyclo[2.2.1]heptan-2-ol (507-70-0) → isobornyl formate (74219-20-8,100101-30-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / diethyl ether / 14 h / 20 °C

2: 91 percent / aq. H₂SO₄

With sulfuric acid; In diethyl ether;

DOI:10.1055/s-1985-31228

upstream raw materials:

formic acid

camphene

d-borneol

dl-camphene

Downstream raw materials:

formic acid

dl-camphene

rac-endo-borneol

1,7,7-trimethyl bicyclo[2.2.1]heptan-2-ol

Refernces