Al(OC₆H₂Bu(t)3-2,4,6)Cl₂ * diethyl ether

Base Information

• Chemical Name: Al(OC₆H₂Bu(t)3-2,4,6)Cl₂ * diethyl ether
• CAS No.: 161531-83-5
• Molecular Formula: C₂₂H₃₉AlCl₂O₂
• Molecular Weight: 433.438
• Mol file: 161531-83-5.mol

Synonyms:

Chemical Property of Al(OC₆H₂Bu(t)3-2,4,6)Cl₂ * diethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Al(OC₆H₂Bu(t)3-2,4,6)Cl₂ * diethyl ether

There total 1 articles about Al(OC₆H₂Bu(t)3-2,4,6)Cl₂ * diethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

aluminium trichloride (7446-70-0) + diethyl ether (60-29-7,927820-24-4) + Li(1+)*OC6H2(C(CH3)3)3(1-)*(C2H5)2O=Li[OC6H2(C(CH3)3)3]*(C2H5)2O → Al(OC6H2Bu(t)3-2,4,6)Cl2 * diethyl ether (161531-83-5)

Guidance literature:

In diethyl ether; byproducts: LiCl; equimolar amts. of AlCl3 and Li-compd., stirring for 20 h at room temp.; solvent removal (vac.), extn. into hexane, concn., crystn. (0°C); elem. anal.;

DOI:10.1039/DT9950000177

Reference yield:

Al(OC6H2Bu(t)3-2,4,6)Cl2 * diethyl ether (161531-83-5) + potassium (7440-09-7) → [Al(OEt)(OC6H2Bu(t)3-2,4,6)2]2

Guidance literature:

byproducts: KCl, Al;

DOI:10.1039/DT9950000177

upstream raw materials:

aluminium trichloride

diethyl ether