3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

Base Information

Chemical Name:3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)
CAS No.:250213-09-3
Molecular Formula:C₁₈H₂₆N₄O₂S₂
Molecular Weight:394.562
Hs Code.:

Synonyms:

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Chemical Property of 3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

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Technology Process of 3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

There total 1 articles about 3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 333-20-0
potassium thioacyanate

: 109-89-7
diethylamine

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 250213-09-3
3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

Guidance literature:: potassium thioacyanate; benzene-1,3-dicarbonyl dichloride; In acetone; for 0.75h; Heating;

diethylamine; In acetone; for 0.75h; Heating;
DOI:10.1039/b509727d

Reference yield: 93.0%

: 53675-30-2
tetrabutylammonium tetrachlorooxorhenate(V)

: 250213-09-3
3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

: [ReOCl(3,3,3',3'-tetraethyl-1,1'-isophthaloylbis(thiourea)^(2-))]n

Guidance literature:: In methanol; to cold soln. (Bu4N)(ReOCl4) in MeOH ligand was added, stirred for 15 min at 10°C; ppt. was filtered off, washed with cold MeOH and dried in vacuo; elem. anal.;
DOI:10.1021/ic1017642

Reference yield:

: 6018-89-9
nickel(II) acetate tetrahydrate

: 250213-09-3
3,3,3′,3′-tetraethyl-1,1-isophthaloylbis(thiourea)

: Ni⁽²⁺⁾*(C₆H₄(C(O)NC(S)N(C₂H₅)2)2)^(2-)=[Ni(C₆H₄(C(O)NC(S)N(C₂H₅)2)2)]

Guidance literature:: In N,N-dimethyl-formamide; byproducts: CH3COOH; rapid combining of warm (50°C) soln. of ligand and warm (50°C) soln. of acetate, vigorous stirring; filtering off ppt., washing several times with H2O, acetone and ether, air-drying;