dimethyl rac-2,5-dibromohexanedioate

Base Information

Chemical Name:dimethyl rac-2,5-dibromohexanedioate
CAS No.:124819-17-6
Molecular Formula:C₈H₁₂Br₂O₄
Molecular Weight:331.989
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl rac-2,5-dibromohexanedioate

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Technology Process of dimethyl rac-2,5-dibromohexanedioate

There total 20 articles about dimethyl rac-2,5-dibromohexanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 868-72-4,53490-47-4,124819-17-6
dimethyl (2R,5S)-2,5-dibromohexanedioate

: 868-72-4,53490-47-4,124819-17-6
dimethyl 2,5-dibromohexanedioate

Guidance literature:: With potassium bromide; In N,N-dimethyl-formamide; at 80 ℃; for 2.3h;
DOI:10.1016/S0957-4166(02)00032-0

Reference yield: 88.0%

: 67-56-1
methanol

: 124-04-9
Adipic acid

: 868-72-4,53490-47-4,124819-17-6
dimethyl 2,5-dibromohexanedioate

Guidance literature:: Adipic acid; With thionyl chloride; at 100 ℃; for 4h;

With bromine; at 20 - 100 ℃; for 22h;

methanol; Inert atmosphere;
DOI:10.1002/chem.201101427

Reference yield: 60.0%

: 67-56-1
methanol

: 7726-95-6
bromine

: 111-50-2
Adipic acid dichloride

: 868-72-4,53490-47-4,124819-17-6
dimethyl rac-2,5-dibromohexanedioate

Guidance literature:: methanol; bromine; Adipic acid dichloride; at 80 ℃; Inert atmosphere; Acidic conditions;

With potassium bromide; at 80 ℃; Inert atmosphere;
DOI:10.1055/s-0033-1338865