N-(p-toluenesulfonyl)dipyridyldiamine

Base Information

Chemical Name:N-(p-toluenesulfonyl)dipyridyldiamine
CAS No.:915202-66-3
Molecular Formula:C₁₇H₁₆N₄O₂S
Molecular Weight:340.406
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(p-toluenesulfonyl)dipyridyldiamine

Chemical Property:

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Technology Process of N-(p-toluenesulfonyl)dipyridyldiamine

There total 1 articles about N-(p-toluenesulfonyl)dipyridyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10201-86-2
(6-amino-2-pyridyl)(2′-pyridyl)amine

: 98-59-9
p-toluenesulfonyl chloride

: 915202-66-3
N-(p-toluenesulfonyl)dipyridyldiamine

Guidance literature:: With pyridine;
DOI:10.1002/ejic.201000145

Reference yield: 74.0%

: 75-09-2
dichloromethane

: 915202-66-3
N-(p-toluenesulfonyl)dipyridyldiamine

: 1243331-00-1
2-(α-pyridylamino)-1,8-naphthyridine

: 540-72-7
sodium thiocyanide

: 6018-89-9
nickel(II) acetate tetrahydrate

: [Ni4(2-(α-pyridylamino)-1,8-naphthyridine(-H))2(N-(p-tolylsulfonyl)dipyridyldiamine(-2H))2(NCS)]*2CH2Cl2

Guidance literature:: With naphthalene; In further solvent(s); Hpyany (0.675 mmol), H2tsdpda (0.675 mmol) and Ni compd. (1.61 mmol) heated in naphthalene at 200°C for 18 h, mixt. cooled to 150°C, NaNCS (3.33 mmol) added, soln. stirred for 2 h; mixt. cooled to 70°C, pptd. (hexane), filtered off, recrystd. (CH2Cl2/hexane), elem. anal.;
DOI:10.1002/ejic.201000145

Reference yield: 67.0%

: 64-17-5
ethanol

: 75-09-2
dichloromethane

: 915202-66-3
N-(p-toluenesulfonyl)dipyridyldiamine

: 1243331-00-1
2-(α-pyridylamino)-1,8-naphthyridine

: 83864-14-6
nickel dichloride

: [Ni4(2-(α-pyridylamino)-1,8-naphthyridine(-H))2(N-(p-tolylsulfonyl)dipyridyldiamine(-2H))2Cl]*0.5CH2Cl2*EtOH

Guidance literature:: With naphthalene; tBuOK; In tert-butyl alcohol; Hpyany (0.675 mmol), H2tsdpda (0.675 mmol) and NiCl2 (1.77 mmol) heated in naphthalene at 200°C for 12 h, tBuOK (2.14 mmol) in tBuOH added dropwise, soln. stirred for 8 h; mixt. cooled to 70°C, pptd. (hexane), filtered off, recrystd. (CH2Cl2/hexane), elem. anal.;
DOI:10.1002/ejic.201000145