Cys-Phe-Arg-Ala-Asn-Lys-OH

Base Information

Chemical Name:Cys-Phe-Arg-Ala-Asn-Lys-OH
CAS No.:1278509-69-5
Molecular Formula:C₃₁H₅₁N₁₁O₈S
Molecular Weight:737.881
Hs Code.:

Synonyms:

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Chemical Property of Cys-Phe-Arg-Ala-Asn-Lys-OH

Chemical Property:

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Technology Process of Cys-Phe-Arg-Ala-Asn-Lys-OH

There total 2 articles about Cys-Phe-Arg-Ala-Asn-Lys-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: fmoc-Lys(Boc)-Wang resin

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: Fmoc-Arg(Pbf)-OH

: 35661-40-6
N-Fmoc L-Phe

: 132388-59-1
L-Asn(Trt)

: 67436-13-9
(R)-3-tert-Butylsulfanyl-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid

: 1278509-69-5
Cys-Phe-Arg-Ala-Asn-Lys-OH

Guidance literature:: fmoc-Lys(Boc)-Wang resin; Wang resin Combinatorial reaction / High throughput screening (HTS);

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; Wang resin Combinatorial reaction / High throughput screening (HTS);

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-Arg(Pbf)-OH; N-Fmoc L-Phe; L-Asn(Trt); (R)-3-tert-Butylsulfanyl-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid; Further stages;
DOI:10.1021/ol402678a

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: Boc-Cys(4-MeBzl)-OH

: 13836-37-8
Boc-Arg(Tos)-OH

: 54613-99-9
Boc-(S)-Lys(2-Cl-Z)-OH

: 65420-40-8
(S)-2-tert-Butoxycarbonylamino-N-(9H-xanthen-9-yl)-succinamic acid

: 1278509-69-5
Cys-Phe-Arg-Ala-Asn-Lys-OH

Guidance literature:: Boc-(S)-Lys(2-Cl-Z)-OH; With HO-CH₂-Pam-polystyrene resin; solid phase reaction;

solid phase reaction;

L-N-Boc-Ala; N-tert-butoxycarbonyl-L-phenylalanine; Boc-Cys(4-MeBzl)-OH; Boc-Arg(Tos)-OH; (S)-2-tert-Butoxycarbonylamino-N-(9H-xanthen-9-yl)-succinamic acid; Further stages;
DOI:10.1002/anie.201105512

Reference yield:

: 1278509-69-5
Cys-Phe-Arg-Ala-Asn-Lys-OH

: LYRAP-S(CH₂)2COOH

: 1356006-89-7
LYRAPCFRANK

: LYRCFRANK

Guidance literature:: With 4-mercaptophenylacetic acid; guanidine hydrochloride; tris-(2-carboxyethyl)-phosphine hydrochloride; sodium hydroxide; In aq. phosphate buffer; at 37 ℃; pH=7.1; Time;
DOI:10.1021/ol402678a