(D,L)-O-ferrocenylmethyl-tyrosine methyl ester

Base Information

Chemical Name:(D,L)-O-ferrocenylmethyl-tyrosine methyl ester
CAS No.:828923-80-4
Molecular Formula:C₂₁H₂₃FeNO₃
Molecular Weight:393.266
Hs Code.:

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Chemical Property of (D,L)-O-ferrocenylmethyl-tyrosine methyl ester

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Technology Process of (D,L)-O-ferrocenylmethyl-tyrosine methyl ester

There total 1 articles about (D,L)-O-ferrocenylmethyl-tyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 828923-54-2,828923-74-6,828923-76-8
(D,L)-O-ferrocenylmethyl-N-(carboxybenzyloxy)tyrosine methyl ester

: 540-69-2
ammonium formate

: 828923-80-4,828923-78-0,828923-55-3
(D,L)-O-ferrocenylmethyl-tyrosine methyl ester

Guidance literature:: With catalyst: Pd-C; In methanol; dichloromethane; under N2; Pd-C and HCO2NH4 added at room temp. to soln. of Fe complex inCH2Cl2-MeOH; stirred at room temp. overnight; filtered over Celite; solvent evapd.; dissolved in AcOEt; washed (brine); aq. phase extd. (AcOEt); combined org. phase washed (H2O); dried (Na2SO4); evapd.; purified by column chromy. (silica gel, AcOEt); elem. anal.;
DOI:10.1016/j.jorganchem.2004.09.049

Reference yield: 76.0%

: 828923-80-4,828923-78-0,828923-55-3
(D,L)-O-ferrocenylmethyl-tyrosine methyl ester

: 67561-03-9
N-benzyloxycarbonylglycinal

: 828923-82-6,828923-84-8,828923-56-4
(C₅H₅)Fe(C₅H₄CH₂OC₆H₄CH₂CH(CO₂CH₃)NHCH₂CH₂NHC(O)OCH₂C₆H₅)

Guidance literature:: With sodium cyanoborohydride; zinc(II) chloride; In methanol; under N2; mixt. of ZnCl2 and NaCNBH3 in dry MeOH added slowly at 0°C into soln. of aminoacetaldehyde and Fe complex in dry MeOH; stirred at room temp. for 18 h; solvent evapd.; taken up with CH2Cl2; washed (aq. NaHCO3); aq. phase extd. (CH2Cl2); combined org. phase washed (H2O); dried (Na2SO4); evapd. invac.; column chromd. (silica gel, light petroleum-AcOEt 3:7);
DOI:10.1016/j.jorganchem.2004.09.049