(Me₂PhP)3RhCl

Base Information

• Chemical Name: (Me₂PhP)3RhCl
• CAS No.: 36103-68-1
• Molecular Formula: C₂₄H₃₃ClP₃Rh
• Molecular Weight: 552.806

Synonyms:

Chemical Property of (Me₂PhP)3RhCl

Chemical Property:

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Technology Process of (Me₂PhP)3RhCl

There total 2 articles about (Me₂PhP)3RhCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhodium(III) chloride trihydrate + ethene (74-85-1) + Dimethyl(phenyl)phosphine (672-66-2) → (Me2PhP)3RhCl (36103-68-1)

Guidance literature:

In ethanol; benzene; by passing C2H4 gas through boiling soln. of Rh salt; addn. of phosphine; evapn.;

Reference yield:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) + Dimethyl(phenyl)phosphine (672-66-2) → (Me2PhP)3RhCl (36103-68-1)

Guidance literature:

In benzene; Rh-complex and phosphine were mixed in benzene; not isolated;

DOI:10.1016/j.jorganchem.2003.09.054

Reference yield: 22.0%

(Me2PhP)3RhCl (36103-68-1) + propionic acid anhydride (123-62-6) → RhCl2(P(C6H5)(CH3)2)2COC2H5 + RhCl2(P(C6H5)(CH3)2)3COC2H5 + RhCl(P(C6H5)(CH3)2)2COC2H5(OOCC2H5)

Guidance literature:

In toluene; (N2); filtered, concd., (31)P-NMR;

DOI:10.1021/om00054a076

upstream raw materials:

ethene

Dimethyl(phenyl)phosphine

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

Downstream raw materials:

Rh{P(CH₃)2(C₆H₅)}4⁽¹⁺⁾*BF₄^(1-)=Rh{P(CH₃)2(C₆H₅)}4(BF₄)

α-Rh(PMe2Ph)3HCl2

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