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C26H24MoN4O3

Base Information
  • Chemical Name:C26H24MoN4O3
  • CAS No.:153606-86-1
  • Molecular Formula:C26H24MoN4O3
  • Molecular Weight:536.442
  • Hs Code.:
C<sub>26</sub>H<sub>24</sub>MoN<sub>4</sub>O<sub>3</sub>

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Chemical Property of C26H24MoN4O3
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Technology Process of C26H24MoN4O3

There total 1 articles about C26H24MoN4O3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In 1,2-dimethoxyethane; byproducts: CO; refluxing a mixt. of ligand and Mo(CO)6 in DME at 85°C for 9 h under N2; removal of solvent under vacuum, recrystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1016/0022-328X(93)83147-N
Guidance literature:
In dichloromethane; addn. of P(OMe)3 to a stirred soln. of Mo-complex dissolved in CH2Cl2, colour changes from orangered to pale yellow, reaction for 6 h; removal of solvent and excess of P(OMe)3 under vac., extn. with hexane, removal under reduced pressure gives Mo-complex, recrystn. of remaining solid residue from CH2Cl2/hexane gives ligand;
DOI:10.1016/0022-328X(93)83147-N
Guidance literature:
In methanol; dichloromethane; addn. of (p-NO2-C6H4N2)Cl to a soln. of Mo-complex dissolved in CH2Cl2 under N2, stirring for 30 min, addn. of NaBPh4 and MeOH, stirring for further 2 h; removal of solvent, recrystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1016/0022-328X(93)83147-N
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