(((C₃H₇)2C₆H₃NCCH₃)2CH)FeCl₂

Base Information

• Chemical Name: (((C₃H₇)2C₆H₃NCCH₃)2CH)FeCl₂
• CAS No.: 445460-76-4
• Molecular Formula: C₂₉H₄₁Cl₂FeN₂
• Molecular Weight: 544.411
• Mol file: 445460-76-4.mol

Synonyms:

Chemical Property of (((C₃H₇)2C₆H₃NCCH₃)2CH)FeCl₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (((C₃H₇)2C₆H₃NCCH₃)2CH)FeCl₂

There total 2 articles about (((C₃H₇)2C₆H₃NCCH₃)2CH)FeCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt + iron(III) chloride (7705-08-0) → (((C3H7)2C6H3NCCH3)2CH)FeCl2 (445460-76-4)

Guidance literature:

In diethyl ether; hexane; toluene; under N2 atm. soln. Li salt ligand in Et2O-hexane was added dropwise to suspn. FeCl3 in toluene; soln. was filtered and cooled to -20°C;

DOI:10.1021/ic025552s

Reference yield:

dichloromethane (75-09-2) + iron(II)β-diketiminate complex (887001-74-3) → (((C3H7)2C6H3NCCH3)2CH)FeCl2 (445460-76-4)

Guidance literature:

at 50 ℃;

DOI:10.1002/chem.201702374

Reference yield:

(((C3H7)2C6H3NCCH3)2CH)FeCl2 (445460-76-4) → C37H60FeN2P

Guidance literature:

Multi-step reaction with 2 steps

1: 20 °C / Inert atmosphere; Schlenk technique

2: toluene / 0.5 h / -30 - -20 °C / Inert atmosphere; Schlenk technique

In toluene;

DOI:10.1002/ejic.201800850

upstream raw materials:

iron(III) chloride

dichloromethane

iron(II)β-diketiminate complex