[Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]

Base Information

Chemical Name:[Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]
CAS No.:673459-85-3
Molecular Formula:C₅₃H₄₇MnN₆O₅
Molecular Weight:902.931
Hs Code.:

[Mn(NO)(piperidine)(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(p-MeOC<sub>6</sub>H<sub>4</sub>)4)]

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Chemical Property of [Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]

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Technology Process of [Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]

There total 1 articles about [Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 110-89-4
piperidine

: 62769-24-8
5,10,15,20-tetra(4-methoxyphenyl) porphyrinato manganese chloride

: 10102-43-9
nitrogen(II) oxide

: 673459-85-3
[Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]

Guidance literature:: In dichloromethane; charging of Schlenk flask with (C20H8N4(p-MeOC6H4)4)MnCl, CH2Cl2 and piperidine; bubbling of NO gas through soln. for 20 min; bubbling of N2 for5 min; addn. of methanol; concn. in vac., pptn., discarding of supernatant soln.; drying in vac.;
DOI:10.1039/b308143p

Reference yield: 77.0%

: 616-47-7
1-methyl-1H-imidazole

: 673459-85-3
[Mn(NO)(piperidine)(C₂₀H₈N₄(p-MeOC₆H₄)4)]

: 673459-88-6
nitrosyl(1-methylimidazole)(tetra-p-methoxyphenylporphirinato^(2-))manganese

Guidance literature:: In dichloromethane; byproducts: piperidine; (N2); using Schlenk techniques; addn. of 1-methylimidazole to stirred soln. of (C20H8N4(MeOC6H4)4)Mn(NO)(piperidine)*0.65CH2Cl2 in CH2Cl2; stirring for 5 h; removal of solvent in vac.; redissolving in CH2Cl2-CH3OH (2:1) mixt., addn. of 1-methylimidazole; slow evapn. of soln. at room temp. under N2; crystn.;
DOI:10.1039/b308143p