Technology Process of (S)-cyclohexyl 2-(dibenzylamino)propanoate
There total 3 articles about (S)-cyclohexyl 2-(dibenzylamino)propanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C
2: sodium hydrogencarbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate;
In
ethyl acetate; acetonitrile;
DOI:10.1039/c1ob06074k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / benzene / 15 h / Reflux; Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C
3: sodium hydrogencarbonate / acetonitrile / 24 h / Reflux; Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid;
In
ethyl acetate; acetonitrile; benzene;
DOI:10.1039/c1ob06074k
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
acetonitrile;
for 24h;
Reflux;
Inert atmosphere;
DOI:10.1039/c1ob06074k