Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

Base Information

Chemical Name:Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester
CAS No.:80065-37-8
Molecular Formula:C₂₇H₃₁NO₁₀S
Molecular Weight:561.61
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

Chemical Property:

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Technology Process of Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

There total 7 articles about Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-32-1
sodium benzoate

: 80065-37-8
Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / aq. ethanol / 48 h / Heating

2: 70 percent / zinc dust, acetic acid / 0.5 h / 70 °C

3: 30 percent / osmium tetroxide, triethylbenzylammonium chloride / CHCl₃; H₂O; 2-methyl-propan-2-ol / 48 h / 60 °C

4: pyridine

With pyridine; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride; acetic acid; zinc; In ethanol; chloroform; water; tert-butyl alcohol;
DOI:10.1246/bcsj.54.2739

Reference yield:

: 69982-70-3,87100-11-6,96291-85-9,115225-41-7
3,4-di-O-acetyl-2,6-dibromo-2,6-dideoxy-5a-carba-β-DL-glucopyranosyl bromide

: 80065-37-8
Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / aq. ethanol / 48 h / Heating

2: 70 percent / zinc dust, acetic acid / 0.5 h / 70 °C

3: 30 percent / osmium tetroxide, triethylbenzylammonium chloride / CHCl₃; H₂O; 2-methyl-propan-2-ol / 48 h / 60 °C

4: pyridine

With pyridine; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride; acetic acid; zinc; In ethanol; chloroform; water; tert-butyl alcohol;
DOI:10.1246/bcsj.54.2739

Reference yield:

: 127-65-1
chloroamine-T

: 80065-37-8
Benzoic acid (1S,2S,3S,4R,5R)-2,3,5-triacetoxy-4-(toluene-4-sulfonylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / osmium tetroxide, triethylbenzylammonium chloride / CHCl₃; H₂O; 2-methyl-propan-2-ol / 48 h / 60 °C

2: pyridine

With pyridine; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; water; tert-butyl alcohol;
DOI:10.1246/bcsj.54.2739