(R)-PhCH(OAc)C(O)OCH₂Et

Base Information

Chemical Name:(R)-PhCH(OAc)C(O)OCH₂Et
CAS No.:85805-90-9
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-PhCH(OAc)C(O)OCH₂Et

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Technology Process of (R)-PhCH(OAc)C(O)OCH₂Et

There total 2 articles about (R)-PhCH(OAc)C(O)OCH₂Et which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71-23-8
propan-1-ol

: 7322-88-5
(S)-acetylmandelic acid

: 85805-90-9
(R)-PhCH(OAc)C(O)OCH₂Et

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -10 ℃;
DOI:10.1039/P29830000083

Reference yield:

: 1122-58-3
dmap

: (+)-(R)-{(η5-C5H5)Re(NO)PPh3(O(CH2)2Me)}

: 29071-09-8
2-acetoxy-2-phenylacetic acid

: 538-75-0
dicyclohexyl-carbodiimide

: (+)-(RR)-{(η5-C5H5)Re(NO)PPh3(OC(O)CH(Ph)O2CCH3)}

: 85805-90-9
(R)-PhCH(OAc)C(O)OCH₂Et

Guidance literature:: In dichloromethane; stirring (0°C, 48 h), warming (room temp.); evapn. of solvent, extn. (benzene), chromy. (silica gel, rthyl acetate/benzene/hexane 5:36: v/v/v and ethyl acetate/hexane 50:50 v/v), pptn. on concn.; elem anal.;