(Ir(N₂C₃(CH₃)2(C₆H₅)C₆H₄)2Cl)2

Base Information

• Chemical Name: (Ir(N₂C₃(CH₃)2(C₆H₅)C₆H₄)2Cl)2
• CAS No.: 1261501-21-6
• Molecular Formula: C₆₈H₆₀Cl₂Ir₂N₈
• Molecular Weight: 1444.62

Synonyms:

Chemical Property of (Ir(N₂C₃(CH₃)2(C₆H₅)C₆H₄)2Cl)2

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Technology Process of (Ir(N₂C₃(CH₃)2(C₆H₅)C₆H₄)2Cl)2

There total 1 articles about (Ir(N₂C₃(CH₃)2(C₆H₅)C₆H₄)2Cl)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iridium(III) chloride hydrate + 4,5-dimethyl-1,2-diphenyl-1H-imidazole (30234-71-0) → (Ir(N2C3(CH3)2(C6H5)C6H4)2Cl)2 (1261501-21-6)

Guidance literature:

In 2-ethoxy-ethanol; water; (Ar) soln. IrCl3*nH2O in 2-ethoxyethanol-water was heated at 60°Cfor 30 min, ligand in 2-ethoxyethanol was added, heated at 120°C overnight; react. mixt. was cooled to r.t., water was added, ppt. was filtered, washed with water and ether and dried;

DOI:10.1021/ic901834v

Reference yield: 50.0%

2-Picolinic acid (98-98-6) + dichloromethane (75-09-2) + (Ir(N2C3(CH3)2(C6H5)C6H4)2Cl)2 (1261501-21-6) → Ir(4,5-dimethyl-1,2-diphenylimidazole(1-))2(pyridine-2-carboxylate)*CH2Cl2

Guidance literature:

With tetrabutylammonium hydroxide; In dichloromethane; (Ar) to soln. Ir complex in CH2Cl2 ligand and Bu4NOH were added, refluxed for 10 h; soln. was cooled to r.t. and evapd. to dryness, residue was dissolved inEtOH, water was added, ppt. was filtered, washed with water and Et2O, d issolved in MeOH, chromy. on Sephadex LH-20 (MeOH); elem. anal.;

DOI:10.1021/ic901834v

Reference yield: 38.0%

(Ir(N2C3(CH3)2(C6H5)C6H4)2Cl)2 (1261501-21-6) + acetylacetone (123-54-6,81235-32-7) → Ir(4,5-dimethyl-1,2-diphenylimidazole(1-))2(acetylacetonate)

Guidance literature:

With tetrabutylammonium hydroxide; In dichloromethane; (Ar) to soln. Ir complex in CH2Cl2 acetylacetone and Bu4NOH were added, refluxed overnight; soln. was cooled to r.t. and evapd. to dryness, residue was dissolved inEtOH, water was added, ppt. was filtered, washed with water and Et2O, d issolved in MeOH, chromy. on Sephadex LH-20 (MeOH); elem. anal.;

DOI:10.1021/ic901834v

upstream raw materials:

4,5-dimethyl-1,2-diphenyl-1H-imidazole

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