Technology Process of Tetrakis[(2-methylphenyl)methyl]stannane
There total 1 articles about Tetrakis[(2-methylphenyl)methyl]stannane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
magnesium;
In
diethyl ether;
react. of organic compound with Mg to form Grignard-soln., addn. of this soln. to a suspn. of SnCl4 in ether, 12 h at room temperature, heating3 h under reflux (under inert gas); addn. of water, removing ether-phase, washing (water, NaCl-soln.), drying (MgSO4), removing solvent, recrystn. (ethylacetate/hexane), elem. anal.;
- Guidance literature:
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mixing at -78°C, heating in sealed ampoule (1 d at 70°C, under inert gas); distn.;