C₉H₁₆BP

Base Information

Chemical Name:C₉H₁₆BP
CAS No.:565232-59-9
Molecular Formula:C₉H₁₆BP
Molecular Weight:166.011
Hs Code.:

Synonyms:

Suppliers and Price of C₉H₁₆BP

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₆BP

Chemical Property:

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Technology Process of C₉H₁₆BP

There total 7 articles about C₉H₁₆BP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 16853-85-3
lithium aluminium tetrahydride

: 13292-87-0
dimethylsulfide borane complex

: 1068-55-9
isopropylmagnesium chloride

: 644-97-3
Dichlorophenylphosphine

: 565232-59-9
trihydro[isopropyl(phenyl)phosphine]boron

Guidance literature:: In diethyl ether; under N2 atm. to soln. PhPCl2 in Et2O at -78°C (i)PrMgCl in Et2O was added, -78°C for 0.5 h, r.t. for 1.5 h, added to suspn. LiAlH4 in Et2O at -78°C, 1 h, quenched with H2O at r.t., BH3*SMe2 was added at 0°C, 0.5 h at r.t.; react. mixt. was poured in mixt. ice and 4M HCl, aq. layer was washed with Et2O, org. phase was dried over MgSO4 and evapd., residue was dissolved in CH2Cl2, filtered through silica and evapd.; elem. anal.;
DOI:10.1002/hlca.200590048

Reference yield: 41.0%

: 1383810-00-1,1383810-02-3,565232-59-9
(R)-(-)-phenyl-i-propylphosphine borane

Guidance literature:: With hydrogenchloride; In toluene; at 20 ℃; Inert atmosphere;

With tert.-butyl lithium; In tetrahydrofuran; hexane; acetic acid; toluene; at -85 ℃; for 0.166667h;