C₁₅H₂₂O₃

Base Information

• Chemical Name: C₁₅H₂₂O₃
• CAS No.: 1197951-70-4
• Molecular Formula: C₁₅H₂₂O₃
• Molecular Weight: 250.338
• Mol file: 1197951-70-4.mol

Synonyms:

Chemical Property of C₁₅H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₂O₃

There total 1 articles about C₁₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

(S)-3-hydroxy-5-methylhexa-2-one (1197951-85-1) + O-(4-methoxybenzyl)-trichloroacetimidate (89238-99-3) → C15H22O3 (1197951-70-4)

Guidance literature:

With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1055/s-0029-1216918

Reference yield:

chloro-trimethyl-silane (75-77-4) + C15H22O3 (1197951-70-4) → C18H30O3Si

Guidance literature:

C₁₅H₂₂O₃; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1.5h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0029-1216918

Reference yield:

C15H22O3 (1197951-70-4) + isobutyraldehyde (78-84-2) → C19H30O4 (1197951-72-6) + C19H30O4 (1197951-74-8)

Guidance literature:

C₁₅H₂₂O₃; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

isobutyraldehyde; In tetrahydrofuran; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1055/s-0029-1216918

upstream raw materials:

(S)-3-hydroxy-5-methylhexa-2-one

O-(4-methoxybenzyl)-trichloroacetimidate

Downstream raw materials:

C₁₉H₃₀O₄

C₁₉H₃₀O₄