2-(2-t-Butoxyethoxy)ethanol

Base Information

• Chemical Name: 2-(2-t-Butoxyethoxy)ethanol
• CAS No.: 110-09-8
• Molecular Formula: C8H18O3
• Molecular Weight: 162.229
• DSSTox Substance ID: DTXSID90436617
• Mol file: 110-09-8.mol

Synonyms:2-(2-t-butoxyethoxy)ethanol;110-09-8;Ethanol, 2-[2-(1,1-dimethylethoxy)ethoxy]-;2-[2-[(2-methylpropan-2-yl)oxy]ethoxy]ethanol;SCHEMBL81017;DTXSID90436617;GICQWELXXKHZIN-UHFFFAOYSA-N;2-(2-(tert-Butoxy)ethoxy)ethanol;AKOS006295068

Chemical Property of 2-(2-t-Butoxyethoxy)ethanol

Chemical Property:

• Vapor Pressure: 0.019mmHg at 25°C
• Boiling Point: 223.498oC at 760 mmHg
• PKA: 14.37±0.10(Predicted)
• Flash Point: 88.969oC
• PSA: 38.69000
• Density: 0.949g/cm3
• LogP: 0.81040
• XLogP3: 0
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 162.125594432
• Heavy Atom Count: 11
• Complexity: 85.8

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)OCCOCCO

Technology Process of 2-(2-t-Butoxyethoxy)ethanol

There total 2 articles about 2-(2-t-Butoxyethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl methyl ether (1634-04-4) + diethylene glycol (111-46-6) → diethylene glycol mono(tert-butyl)ether (110-09-8) + 2-[2-(2-tert-butoxyethoxy)ethoxy]-2-methylpropane (107-79-9)

Guidance literature:

With [H⁺] cation exchange resin (Amberlyst 15); at 70 ℃; for 6h; Temperature; Autoclave;

Reference yield:

isobutene (115-11-7,15220-85-6) + diethylene glycol (111-46-6) → diethylene glycol mono(tert-butyl)ether (110-09-8) + 2-[2-(2-tert-butoxyethoxy)ethoxy]-2-methylpropane (107-79-9)

Guidance literature:

Amberlyst 15; at 50 ℃; for 6h; under 10343.2 Torr; Product distribution / selectivity;

Reference yield: 94.2%

maleic anhydride (108-31-6) + diethylene glycol mono(tert-butyl)ether (110-09-8) → C20H36O8

Guidance literature:

With KC₁₀₅A strong acid catalyst; In toluene; at 100 ℃; for 5h; Inert atmosphere; Flow reactor;

upstream raw materials:

isobutene

diethylene glycol

tert-butyl methyl ether

Downstream raw materials:

diethylene glycol methyl tert-butyl ether

Refernces

• 1、 -. "Method of Producing Diethylene-Glycol Tert-Butyl Ether Using Isobutylene and Diethylene Glycol". Page/Page column 2-3; sheet 2. . Retrieved 2011/07/08.