Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester

Base Information

• Chemical Name: Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester
• CAS No.: 192060-78-9
• Molecular Formula: C₈₈H₁₂₈O₂₀P₄S₄
• Molecular Weight: 1758.13

Synonyms:

Chemical Property of Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester

Chemical Property:

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Technology Process of Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester

There total 1 articles about Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dipalmitoyl-sn-glycerol (30334-71-5) + Thiophosphoric acid O,O'-dibenzyl ester O''-[(1S,2R,3R,4S,5R,6S)-2,3-bis-(bis-benzyloxy-thiophosphoryloxy)-5-(diisopropylamino-methoxy-phosphanyloxy)-4,6-bis-methoxymethoxy-cyclohexyl] ester → Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester (192060-78-9)

Guidance literature:

With 1H-tetrazole; sulfur; Multistep reaction;

DOI:10.1016/S0960-894X(97)00196-0

Reference yield:

chloro-trimethyl-silane (75-77-4) + Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester (192060-78-9) → C66H146O20P4S4Si7

Guidance literature:

With trimethylamine; at 23 ℃; for 240h;

DOI:10.1016/S0960-894X(97)00196-0

Reference yield:

Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-{methoxy-[(1R,2S,3S,4R,5R,6S)-3,4,5-tris-(bis-benzyloxy-thiophosphoryloxy)-2,6-bis-methoxymethoxy-cyclohexyloxy]-thiophosphoryloxy}-ethyl ester (192060-78-9) → C66H104O20P4S4(4-)

Guidance literature:

With trimethylamine;

DOI:10.1016/S0960-894X(97)00196-0

upstream raw materials:

1,2-dipalmitoyl-sn-glycerol

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