1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

Base Information

Chemical Name:1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride
CAS No.:958293-11-3
Molecular Formula:C₁₆H₂₂N₃O*Cl
Molecular Weight:307.823
Hs Code.:

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Chemical Property of 1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

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Technology Process of 1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

There total 1 articles about 1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4238-71-5
1-benzylimidazole

: 15678-99-6
N-tert-butylchloroacetamide

: 958293-11-3
1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

Guidance literature:: In toluene; at 110 ℃; for 12h;
DOI:10.1039/b706607d

Reference yield: 66.0%

: 958293-11-3
1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

: 75-09-2
dichloromethane

: 20667-12-3
silver(l) oxide

: [(1-(benzyl)-3-(N-tert-butylacetamido)imidazol-2-ylidene)AgCl]*0.5CH₂Cl₂

Guidance literature:: In dichloromethane; std. Schlenk technique; mixt. of chloride and Ag2O in CH2Cl2 was stirredat room temp. for 6 h; filtered; solvent removed (vac.); elem. anal.;
DOI:10.1021/ic701830m

Reference yield: 40.0%

: 110-86-1
pyridine

: 958293-11-3
1-(benzyl)-3-(N-tert-butylacetamido)imidazolium chloride

: 75-09-2
dichloromethane

: palladium dichloride

: trans-[1-(benzyl)-3-(N-t-butylacetamido)imidazol-2-ylidene]Pd(pyridine) dichloride*0.5(dichloromethane)

Guidance literature:: With K₂CO₃; In pyridine; (glovebox, Schlenk); mixt. of ligand, PdCl2, K2CO3 refluxed in pyridine for 16 h; filtered, solvent removed under vac., residue washed with aq. soln. of CuSO4, aq. layer extd. with CH2Cl2, organic layer collected, solvent removed under vac.; elem. anal.;
DOI:10.1039/b706607d