(t)BuC(NCy)2GaMe₂

Base Information

Chemical Name:(t)BuC(NCy)2GaMe₂
CAS No.:213386-23-3
Molecular Formula:C₁₉H₃₇GaN₂
Molecular Weight:363.239
Hs Code.:

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Chemical Property of (t)BuC(NCy)2GaMe₂

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Technology Process of (t)BuC(NCy)2GaMe₂

There total 1 articles about (t)BuC(NCy)2GaMe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: Li[((t)BuC(N(cyclohexyl))2)]

: 676-58-4
methylmagnesium chloride

: 13450-90-3
Gallium trichloride

: 213386-23-3
(t)BuC(NCy)2GaMe₂

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: LiCl; N2-atmosphere; addn. of soln. of GaCl3 to suspension of ligand at -78°C (Et2O), warming to room temp., stirring for 12 h, cooling to -78°C, addn. of Grignard reagent (THF), stirring at room temp. for 15h; evapn., extn. (hexanes), concn., crystn. on standing at -78°C, collection (filtration); elem. anal.;
DOI:10.1021/om990472q