Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

Base Information

Chemical Name:Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)
CAS No.:476015-01-7
Molecular Formula:C₃₆H₃₆ClNP₂Pd
Molecular Weight:686.509
Hs Code.:

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Chemical Property of Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

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Technology Process of Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

There total 1 articles about Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 64406-71-9
[1,1'-bis(diphenylphosphino)ethane(Pd(CH3)Cl)]

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 476015-01-7
Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In tetrahydrofuran; (N2); addn. of isocyanide to a soln. of palladium complex in THF, stirring for 2 h; evapn., washing with Et2O, cold THF; elem. anal.;
DOI:10.1021/om020444z

Reference yield: 90.0%

: 14104-20-2
silver tetrafluoroborate

: 75-09-2
dichloromethane

: 476015-01-7
Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

: 109-90-0
ethyl isocyanate

: [Pd(C(CH₂)N(Xy)C(O)NHEt)(1,2-bis(diphenylphosphino)ethane)][BF₄]*0.5(dichloromethane)

Guidance literature:: In dichloromethane; byproducts: AgCl; under N2; EtNCO (1.1 equiv.) added to stirring soln. of Pd complex in CH2Cl2; AgBF4 (1 equiv.) added as solid; stirred for 10 min; filtered; filtrate concd. under reduced pressure; pptd. by addition of hexane; elem. anal.;
DOI:10.1021/om030493r

Reference yield: 83.0%

: tetrafluoroboric acid

: 476015-01-7
Pd(C(Me)=NXy)(Cl)(1,2-bis(diphenylphosphino)ethane)

: [Pd(C(Me)=NHXy)(Cl)(1,2-bis(diphenylphosphino)ethane)][BF₄]

Guidance literature:: In diethyl ether; dichloromethane; under N2; Pd complex dissolved in CH2Cl2; HBF4 in Et2O added dropwise; filtered; solvent removed under reduced pressure from filtrate; stirred rapidly with Et2O; elem. anal.;
DOI:10.1021/om030493r