1-Benzoyl-4-phenylsemicarbazide

Base Information

• Chemical Name: 1-Benzoyl-4-phenylsemicarbazide
• CAS No.: 1152-32-5
• Molecular Formula: C14H13N3O2
• Molecular Weight: 255.276
• Hs Code.: 2928000090
• European Community (EC) Number: 621-476-1
• DSSTox Substance ID: DTXSID50351514
• Nikkaji Number: J2.179.003F
• Wikidata: Q82127981
• Mol file: 1152-32-5.mol

Synonyms:1-Benzoyl-4-phenylsemicarbazide;1152-32-5;2-benzoyl-N-phenylhydrazinecarboxamide;1-benzamido-3-phenylurea;N-[(phenylcarbamoyl)amino]benzamide;Maybridge1_006757;CBDivE_013351;SCHEMBL12305515;HMS560L03;DTXSID50351514;WPMMTXFVYJICDR-UHFFFAOYSA-N;MFCD00088033;STK414202;AKOS001198253;2-Benzoyl-N-phenylhydrazine-1-carboxamide;CS-0329541;FT-0633408;N-phenyl-2-(phenylcarbonyl)hydrazinecarboxamide;AB00078515-01;Benzoic acid, 2-[(phenylamino)carbonyl]hydrazide;A803393;Z44592185

Chemical Property of 1-Benzoyl-4-phenylsemicarbazide

Chemical Property:

• Melting Point: 220-222oC
• PSA: 70.23000
• Density: 1.279g/cm3
• LogP: 3.00790
• XLogP3: 2
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 255.100776666
• Heavy Atom Count: 19
• Complexity: 308

Purity/Quality:

97% ^*data from raw suppliers

1-Benzoyl-4-phenylsemicarbazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NNC(=O)NC2=CC=CC=C2

Technology Process of 1-Benzoyl-4-phenylsemicarbazide

There total 8 articles about 1-Benzoyl-4-phenylsemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-phenyl-3H-[1,3,4]oxadiazol-2-one (1199-02-6) + aniline (62-53-3) → 1-benzoyl-4-phenylsemicarbazide (1152-32-5)

Guidance literature:

In various solvent(s); at 70 ℃; for 48h;

Reference yield: 96.0%

phenyl isocyanate (103-71-9) + benzoic acid hydrazide (613-94-5) → 1-benzoyl-4-phenylsemicarbazide (1152-32-5)

Guidance literature:

In benzene; for 1.5h; Heating;

Reference yield:

ethyl nitrite (109-95-5) + benzoic acid hydrazide (613-94-5) → 1-benzoyl-4-phenylsemicarbazide (1152-32-5) + N'-benzoylbenzohydrazide (787-84-8)

Guidance literature:

With ethanol;

upstream raw materials:

phenyl isocyanate

benzoic acid hydrazide

benzene

ethyl nitrite

Downstream raw materials:

2-phenylamino-5-phenyl-1,3,4-oxadiazole

benzoic acid hydrazide

bis(diphenyl)urea

carbon dioxide