tetrakisbenzonitrile copper(I) tetrafluoroborate

Base Information

Chemical Name:tetrakisbenzonitrile copper(I) tetrafluoroborate
CAS No.:49731-93-3
Molecular Formula:BF₄*C₂₈H₂₀CuN₄
Molecular Weight:562.844
Hs Code.:

Synonyms:

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Chemical Property of tetrakisbenzonitrile copper(I) tetrafluoroborate

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Technology Process of tetrakisbenzonitrile copper(I) tetrafluoroborate

There total 1 articles about tetrakisbenzonitrile copper(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: copper(I) oxide

: tetrafluoroboric acid

: 100-47-0
benzonitrile

: 49731-93-3
tetrakisbenzonitrile copper(I) tetrafluoroborate

Guidance literature:: In benzonitrile; (Ar); Cu2O suspd. in benzonitrile; 40% soln. of HBF4 added at once undercontinuous stirring; stirred for 1 h; toluene added; filtered off; washed with Et2O; dried in vacuum; elem. anal.;
DOI:10.1016/j.poly.2007.04.007

Reference yield: 92.0%

: 75-09-2
dichloromethane

: 49731-93-3
tetrakisbenzonitrile copper(I) tetrafluoroborate

: 1372802-37-3
N,N'-bis(4-isopropylphenyl)acenaphthenequinonediimine

: 603-35-0
triphenylphosphine

: [Cu(N,N'-bis(4-isopropylphenyl)acenaphthenequinonediimine)(PPh₃)2]BF₄*0.5(dichloromethane)

Guidance literature:: In dichloromethane; a suspn. of Cu complex and P(C6H5)3 stirred for 2 h at room temp., treated with a soln. of C12H6(NC6H4CH(CH3)2)2, stirred for 2 h; filtered, concd. (vac.), layered with pentane, crystd. at -20°C, filtered, washed (pentane), dried (vac.); elem. anal.;
DOI:10.1039/c2dt11854h

Reference yield: 67.0%

: 49731-93-3
tetrakisbenzonitrile copper(I) tetrafluoroborate

: 153625-67-3
1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene

: 1372802-34-0
[Cu(N,N'-bis(2,6-diisopropylphenyl)acenaphthenequinonediimine)(PhCN)2]BF₄

Guidance literature:: In dichloromethane; a suspn. of Cu complex treated with a soln. of ligand at room temp., stirred overnight; filtered, concd. (vac.), layered with pentane, crystd. at -20°C, filtered, washed (pentane), dried (vac.); elem. anal.;
DOI:10.1039/c2dt11854h