iPr₂NC(CyN)2AlCl₂

Base Information

Chemical Name:iPr₂NC(CyN)2AlCl₂
CAS No.:1239598-48-1
Molecular Formula:C₁₉H₃₆AlCl₂N₃
Molecular Weight:404.402
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Chemical Property of iPr₂NC(CyN)2AlCl₂

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Technology Process of iPr₂NC(CyN)2AlCl₂

There total 1 articles about iPr₂NC(CyN)2AlCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 7446-70-0
aluminium trichloride

: 538-75-0
dicyclohexyl-carbodiimide

: 4111-54-0
lithium diisopropyl amide

: 1239598-48-1
iPr₂NC(CyN)2AlCl₂

Guidance literature:: In diethyl ether; hexane; byproducts: LiCl; (N2); using Schlenk techniques; cooling of slurry of LiN(i-Pr)2/Et2O to -78°C, addn. soln. of (CyN)2C/Et2O, warming to room temp., stirring for 1 h, cooling to -78°C, addn. of AlCl3 soln. in C6H14, warming to room temp., stirring for 18 h; filtration, removal of volatiles in vac., recrystn. from toluene at -35°C, filtration; elem. anal.;
DOI:10.1021/om100278b