lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)

Base Information

Chemical Name:lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)
CAS No.:943331-67-7
Molecular Formula:C₁₂H₂₃CuNOSi*Li
Molecular Weight:295.893
Hs Code.:

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Chemical Property of lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)

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Technology Process of lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)

There total 2 articles about lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-68-7
cyclohexenone

: Li(dimethylcuprate)*LiI

: 7677-24-9
trimethylsilyl cyanide

: 943331-67-7
lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)

Guidance literature:: In tetrahydrofuran-d8; addn. of soln. of C6H8O in THF-d8 to a soln. of Me2CuLi*LiI in THF-d8 at-100 °C, addn. of THF-d8 soln. of Me3SiCN; not isolated, NMR anal.;
DOI:10.1021/ja067533d

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 930-68-7
cyclohexenone

: Me₂CuLi*LiCN

: 943331-67-7
lithium cyanobis(methyl)(3-trimethylsiloxycyclohex-2-en-1-yl)cuprate(III)

Guidance literature:: In tetrahydrofuran-d8; addn. of soln. of Me3SiCl in THF-d8 to a soln. of Me2CuLi*LiCN in THF-d8at -100 °C, addn. of THF-d8 soln. of C6H8O; not isolated, NMR anal.;
DOI:10.1021/ja067533d