N~1~,N~2~-di(tert-butyl)-N'~1~,N'~2~-diphenylethanediimidamide

Base Information

• Chemical Name: N~1~,N~2~-di(tert-butyl)-N'~1~,N'~2~-diphenylethanediimidamide
• CAS No.: 121264-09-3
• Molecular Formula: C22H30N4
• Molecular Weight: 350.50000
• Mol file: 121264-09-3.mol

Synonyms:Ethanediimidamide,N,N''-bis(1,1-dimethylethyl)-N',N'''-diphenyl;

Chemical Property of N~1~,N~2~-di(tert-butyl)-N'~1~,N'~2~-diphenylethanediimidamide

Chemical Property:

• PSA: 48.78000
• LogP: 5.87770

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N~1~,N~2~-di(tert-butyl)-N'~1~,N'~2~-diphenylethanediimidamide

There total 1 articles about N~1~,N~2~-di(tert-butyl)-N'~1~,N'~2~-diphenylethanediimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N,N'-diphenyloxaldiimidoyl dichloride (20033-74-3) + tert-butylamine (75-64-9) → C22H30N4 (121264-09-3)

Guidance literature:

In toluene; at 20 ℃; for 48h;

DOI:10.1039/b010017j

Reference yield: 82.0%

tetrakis(dimethylamido)zirconium (IV) (19756-04-8) + (C6H5NCNHC(CH3)3)2 (121264-09-3) → [(C6H5NCNC(CH3)3)Zr(N(CH3)2)3]2 (355806-73-4)

Guidance literature:

In toluene; (N2); addn. of a soln. of ligand in toluene to a soln. of zirconium compd. in toluene at room temp., heating to 85°C for 3 h; filtration, evapn., washing with pentane; elem. anal.;

DOI:10.1039/b010017j

Reference yield: 80.0%

chloro-trimethyl-silane (75-77-4) + C22H30N4 (121264-09-3) → C28H46N4Si2

Guidance literature:

C₂₂H₃₀N₄; With n-butyllithium; In diethyl ether; at 0 - 20 ℃; for 3h;

chloro-trimethyl-silane; In tetrahydrofuran; at 75 ℃; for 8h; Further stages.;

DOI:10.1039/b010017j

upstream raw materials:

N,N'-diphenyloxaldiimidoyl dichloride

tert-butylamine

Downstream raw materials:

C₆H₅NCNHC(CH₃)3C(NC(CH₃)3)NC₆H₅TaCl₃N(CH₂CH₃)2

[(C₆H₅NCNC(CH₃)3)Zr(N(CH₃)2)3]2

[(C₆H₅NCNC(CH₃)3)Ti(N(CH₃)2)3]2