cyclo

Base Information

• Chemical Name: cyclo
• CAS No.: 52661-96-8
• Molecular Formula: C₉H₁₄N₂O₄
• Molecular Weight: 214.221

Synonyms:

Chemical Property of cyclo

Chemical Property:

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Technology Process of cyclo

There total 5 articles about cyclo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(N-benzyloxycarbonyl-glycyl)-L-glutamic acid diethyl ester (3369-03-7) → cyclo (52661-96-8)

Guidance literature:

With palladium on activated charcoal; ethanol; Hydrogenation;

DOI:10.1557/JMR.2002.0375

Reference yield:

N-chloroacetyl-L-glutamic acid diethyl ester (76385-54-1) → cyclo (52661-96-8)

Guidance literature:

With ammonia; at 100 ℃;

Reference yield:

L-glutamic acid diethyl ester (16450-41-2) → cyclo (52661-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂CO₃

2: aq.-ethanolic NH₃ / 100 °C

With ammonia; sodium carbonate;

upstream raw materials:

N-chloroacetyl-L-glutamic acid diethyl ester

ethanol

Glycylglutamic acid

N-(N-benzyloxycarbonyl-glycyl)-L-glutamic acid diethyl ester

Downstream raw materials:

acide 3-(3,6-dioxopiperazin-2-yl)-propanoique

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