BUTTPARK 17\01-09

Base Information

• Chemical Name: BUTTPARK 17\01-09
• CAS No.: 154877-60-8
• Molecular Formula: C₁₀H₉ClN₂O
• Molecular Weight: 208.647
• Hs Code.: 2933998090
• Mol file: 154877-60-8.mol

Synonyms:

Chemical Property of BUTTPARK 17\01-09

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1-(6-CHLORO-2-METHYLIMIDAZO[1,2-A]PYRIDIN-3-YL)-1-ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of BUTTPARK 17\01-09

There total 3 articles about BUTTPARK 17\01-09 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

5-chloro-2-pyridylamine (1072-98-6) + acetylacetone (123-54-6,81235-32-7) → 1-(6-chloro-2-methylimidazo[1,2-a]pyridin-3-yl)ethanone (154877-60-8)

Guidance literature:

With [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; In tetrahydrofuran; at 7 ℃;

DOI:10.1055/s-0030-1260106

Reference yield: 42.0%

5-chloro-2-pyridylamine (1072-98-6) + 3-chloropentane-2,4-dione (1694-29-7) → 1-(6-chloro-2-methylimidazo[1,2-a]pyridin-3-yl)ethanone (154877-60-8)

Guidance literature:

In ethanol; for 10h; Heating;

DOI:10.1016/j.bmc.2006.09.047

Reference yield: 38.0%

→ 1-(6-chloro-2-methylimidazo[1,2-a]pyridin-3-yl)ethanone (154877-60-8)

Guidance literature:

In ethanol; for 10h; Reflux;

upstream raw materials:

5-chloro-2-pyridylamine

3-chloropentane-2,4-dione

acetylacetone

Downstream raw materials:

3-[4-(6-Chloro-2-methyl-imidazo[1,2-a]pyridin-3-yl)-thiazol-2-ylamino]-4-isopropoxy-benzamide

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