Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)-

Base Information

Chemical Name:Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)-
CAS No.:124083-18-7
Molecular Formula:C15H21ClO3
Molecular Weight:284.783
Hs Code.:
Mol file:124083-18-7.mol

Synonyms:

Suppliers and Price of Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)-

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)-

There total 8 articles about Oxiranemethanol, 2-[6-(4-chlorophenoxy)hexyl]-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82258-37-5
ethyl 2-[6-(p-chlorophenoxy)hexyl]acrylate

: 124083-18-7
{(S)-2-[6-(4-Chloro-phenoxy)-hexyl]-oxiranyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: aluminium trihydride / diethyl ether

2: 49 percent / t-butylhydroperoxide, titanium isopropoxide, diethyl L-(+)-tartrate / -20 deg C, 3 h. then room temp., 1 h.

With aluminium hydride; titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; In diethyl ether;
DOI:10.1016/S0040-4039(01)80643-2

Reference yield:

: 124083-17-6
8-(4-Chloro-phenoxy)-2-methylene-octanoic acid

: 124083-18-7
{(S)-2-[6-(4-Chloro-phenoxy)-hexyl]-oxiranyl}-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / SOCl₂ / 18 h / from 0 deg C to room temp.

2: 60 percent / NaBH₄-silica / diethyl ether / 18 h / Ambient temperature

3: 49 percent / t-butylhydroperoxide, titanium isopropoxide, diethyl L-(+)-tartrate / -20 deg C, 3 h. then room temp., 1 h.

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; thionyl chloride; diethyl (2R,3R)-tartrate; silica gel; In diethyl ether;
DOI:10.1016/S0040-4039(01)80643-2

Reference yield:

: 124083-16-5
8-(4-Chloro-phenoxy)-2-methylene-octanoyl chloride

: 124083-18-7
{(S)-2-[6-(4-Chloro-phenoxy)-hexyl]-oxiranyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaBH₄-silica / diethyl ether / 18 h / Ambient temperature

2: 49 percent / t-butylhydroperoxide, titanium isopropoxide, diethyl L-(+)-tartrate / -20 deg C, 3 h. then room temp., 1 h.

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; diethyl (2R,3R)-tartrate; silica gel; In diethyl ether;
DOI:10.1016/S0040-4039(01)80643-2