Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Base Information

Chemical Name:Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester
CAS No.:192060-74-5
Molecular Formula:C₆₈H₇₇O₁₄P₃Si
Molecular Weight:1239.36
Hs Code.:

Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Synonyms:

Suppliers and Price of Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

There total 7 articles about Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 331679-26-6
2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

: 192060-74-5
Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / imidazole

2: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3: 92 percent / pyridine / -40 °C

4: 75 percent / diisopropylethylamine / dimethylformamide

5: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

6: tetrazole

With pyridine; 1H-imidazole; 1H-tetrazole; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; methylamine; 2-hydroxyethanethiol; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo0206418

Reference yield:

: 142534-54-1
1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol

: 192060-74-5
Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / pyridine / -40 °C

2: 75 percent / diisopropylethylamine / dimethylformamide

3: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

4: tetrazole

With pyridine; 1H-tetrazole; N-ethyl-N,N-diisopropylamine; methylamine; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo0206418

Reference yield:

: 142563-77-7
1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-3,4,5-O-trisbenzoyl-myo-inositol

: 192060-74-5
Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

2: tetrazole

With 1H-tetrazole; methylamine; In ethanol; chloroform;
DOI:10.1021/jo0206418