1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol

Base Information

• Chemical Name: 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol
• CAS No.: 142534-58-5
• Molecular Formula: C₂₆H₃₈O₈Si
• Molecular Weight: 506.668

Synonyms:1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol

Chemical Property of 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol

There total 11 articles about 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-3,4,5-O-trisbenzoyl-myo-inositol (142563-77-7) → 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol (142534-58-5)

Guidance literature:

With methylamine; In ethanol; chloroform; at 50 ℃; for 48h;

DOI:10.1021/jo0206418

Reference yield:

1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol (142534-54-1) → 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol (142534-58-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / pyridine / -40 °C

2: 75 percent / diisopropylethylamine / dimethylformamide

3: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

With pyridine; N-ethyl-N,N-diisopropylamine; methylamine; In ethanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1021/jo0206418

Reference yield:

1D-1-O-(tert-butyldiphenylsilyl)-3,4,5-O-trisbenzoyl-myo-inositol (142534-57-4) → 1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol (142534-58-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / diisopropylethylamine / dimethylformamide

2: 96 percent / methylamine / CHCl₃; ethanol / 48 h / 50 °C

With N-ethyl-N,N-diisopropylamine; methylamine; In ethanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1021/jo0206418

upstream raw materials:

1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-3,4,5-O-trisbenzoyl-myo-inositol

2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol

1D-1-O-(tert-butyldiphenylsilyl)-3,4,5-O-trisbenzoyl-myo-inositol

Downstream raw materials:

Phosphorous acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphanyloxy)-4-(tert-butyl-diphenyl-silanyloxy)-3,5-bis-methoxymethoxy-cyclohexyl ester

1D-1-O-(tert-butyldiphenylsilyl)-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

1D-2,6-O-bis(methoxymethylene)-myo-inositol 3,4,5-tris(dibenzyl phosphate)

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