bis(cupferronato)copper(II)

Base Information

Chemical Name:bis(cupferronato)copper(II)
CAS No.:52079-21-7
Molecular Formula:C₁₂H₁₀CuN₄O₄
Molecular Weight:337.782
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(cupferronato)copper(II)

Chemical Property:

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Technology Process of bis(cupferronato)copper(II)

There total 3 articles about bis(cupferronato)copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: copper(II) oxide

: 15613-15-7,52079-21-7
Cu(C₆H₅N₂O₂)2

Guidance literature:: With Mg; NO; phenyl halide; In diethyl ether; water; slow addn. of phenylhalide to Mg in ether; refluxing (1h); cooling; addn. of NO into evacuated flask; stirring; removal of solvent; dissolving of dried NO-Grignard in H2O; addn. of aq. H2SO4; extn. into ether; stirring of extract with CuO for several h;; suspn. was stored overnight; excess of CuO was filtered off and washed with acetone; filtrate and acetone washings were combined and evapd. to dryness; recrystn. from methylated spirits; dried under vac.;;
DOI:10.1016/S0277-5387(00)80898-0

Reference yield:

: cupferron

: 7758-99-8
copper(II) sulfate

: 15613-15-7,52079-21-7
Cu(C₆H₅N₂O₂)2

Guidance literature:: In water;

Reference yield:

: cupferron

: 6046-93-1
copper(II) acetate monohydrate

: 52079-21-7,15613-15-7
bis(cupferronato)copper(II)

Guidance literature:: In methanol; acetonitrile; Cu(CH3COO)2 in MeOH addn. to cupferron in CH3CN, refluxing for 4 d;
DOI:10.1107/S0108270195002770