CH₃OCH₂C[CH₂(C₃H₃N₂)]2[CH₂P(C₆H₅)2]NiP(C₆H₅)3(CH₃)3C₆H₂⁽¹⁺⁾*PF₆^(1-)=CH₃OCH₂C[CH₂(C₃H₃N₂)]2CH₂P₂(C₆H₅)5Ni(CH₃)3C₆H₂PF₆

Base Information

• Chemical Name: CH₃OCH₂C[CH₂(C₃H₃N₂)]2[CH₂P(C₆H₅)2]NiP(C₆H₅)3(CH₃)3C₆H₂⁽¹⁺⁾*PF₆^(1-)=CH₃OCH₂C[CH₂(C₃H₃N₂)]2CH₂P₂(C₆H₅)5Ni(CH₃)3C₆H₂PF₆
• CAS No.: 623125-62-2
• Molecular Formula: C₅₁H₅₃N₄NiOP₂*F₆P
• Molecular Weight: 1003.61

Synonyms:

Chemical Property of CH₃OCH₂C[CH₂(C₃H₃N₂)]2[CH₂P(C₆H₅)2]NiP(C₆H₅)3(CH₃)3C₆H₂⁽¹⁺⁾*PF₆^(1-)=CH₃OCH₂C[CH₂(C₃H₃N₂)]2CH₂P₂(C₆H₅)5Ni(CH₃)3C₆H₂PF₆

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Technology Process of CH₃OCH₂C[CH₂(C₃H₃N₂)]2[CH₂P(C₆H₅)2]NiP(C₆H₅)3(CH₃)3C₆H₂⁽¹⁺⁾*PF₆^(1-)=CH₃OCH₂C[CH₂(C₃H₃N₂)]2CH₂P₂(C₆H₅)5Ni(CH₃)3C₆H₂PF₆

There total 1 articles about CH₃OCH₂C[CH₂(C₃H₃N₂)]2[CH₂P(C₆H₅)2]NiP(C₆H₅)3(CH₃)3C₆H₂⁽¹⁺⁾*PF₆^(1-)=CH₃OCH₂C[CH₂(C₃H₃N₂)]2CH₂P₂(C₆H₅)5Ni(CH₃)3C₆H₂PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

thallium(I) hexafluorophosphate (60969-19-9) + trans-(bromomesityl)bis(triphenylphosphino)nickel(II) + dichloromethane (75-09-2) + 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether (623124-95-8) → CH3OCH2C[CH2(C3H3N2)]2[CH2P(C6H5)2]NiP(C6H5)3(CH3)3C6H2(1+)*PF6(1-)=CH3OCH2C[CH2(C3H3N2)]2CH2P2(C6H5)5Ni(CH3)3C6H2PF6 (623125-62-2)

Guidance literature:

In tetrahydrofuran; toluene; byproducts: TlBr; (Ar); ligand in toluene added to Ni complex in toluene, stirred at 25°C for 10 h, evapd.(vac.), dissolved (THF), treated with solid TlPF6, stirred at 25°C for 3 h; filtered, evapd.(vac.), suspnd.(petroleum ether), filtered, washed (petroleum ether), dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;

DOI:10.1002/ejic.200200535

upstream raw materials:

thallium(I) hexafluorophosphate

dichloromethane

3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether

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