Cu(OC₆H₅)2(H₂NCH₂CH₂NH₂)*C₆H₅OH

Base Information

• Chemical Name: Cu(OC₆H₅)2(H₂NCH₂CH₂NH₂)*C₆H₅OH
• CAS No.: 71851-76-8
• Molecular Formula: C₆H₆O*C₁₄H₁₈CuN₂O₂
• Molecular Weight: 403.968
• Mol file: 71851-76-8.mol

Synonyms:

Chemical Property of Cu(OC₆H₅)2(H₂NCH₂CH₂NH₂)*C₆H₅OH

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of Cu(OC₆H₅)2(H₂NCH₂CH₂NH₂)*C₆H₅OH

There total 2 articles about Cu(OC₆H₅)2(H₂NCH₂CH₂NH₂)*C₆H₅OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(1,2-ethanediamine)Cu(II) dichloride (22980-84-3) + Na(1+)*OC6H5(1-)*C6H5OH=NaOC6H5*C6H5OH → Cu(OC6H5)2(H2NCH2CH2NH2)*C6H5OH (71851-76-8)

Guidance literature:

In tetrahydrofuran; byproducts: NaCl, phenol; absence of air and moisture; addn. of 2 equiv phenolate to Cu-complex; filtration (after 1.5 h), concn. of filtrate (reduced pressure), crystn.(refrigerator), filtration, drying (vac.); elem. anal.;

DOI:10.1039/DT9790001238

Reference yield:

copper(II) acetate monohydrate (6046-93-1) + ethylenediamine (107-15-3,85404-18-8) + phenol (108-95-2,27073-41-2) → Cu(OC6H5)2(H2NCH2CH2NH2)*C6H5OH (71851-76-8)

Guidance literature:

With sodium hydroxide; In water; preparation by method similar to: Calderazzo, F. et al., J. Chem. Soc., Dalton Trans., 1980, 1419; elem. anal.;

DOI:10.1246/bcsj.70.2167

upstream raw materials:

(1,2-ethanediamine)Cu(II) dichloride

copper(II) acetate monohydrate

ethylenediamine

phenol