CoEt(pyridine)(dithiophenylglyoxime(-1H))2

Base Information

Chemical Name:CoEt(pyridine)(dithiophenylglyoxime(-1H))2
CAS No.:1159404-40-6
Molecular Formula:C₃₅H₃₂CoN₅O₄S₄
Molecular Weight:773.927
Hs Code.:

Synonyms:

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Chemical Property of CoEt(pyridine)(dithiophenylglyoxime(-1H))2

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Technology Process of CoEt(pyridine)(dithiophenylglyoxime(-1H))2

There total 4 articles about CoEt(pyridine)(dithiophenylglyoxime(-1H))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1313442-69-1
CoCl(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1313442-71-5
CoEt(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1159404-40-6
CoEt(pyridine)(dithiophenylglyoxime(-1H))2

Guidance literature:: With NaBH₄; In not given; reacted for 15 min;
DOI:10.1016/j.jorganchem.2011.02.033

Reference yield:

: 74-96-4
ethyl bromide

: 1159404-38-2
CoCl((bis(thiophenyl)glyoxime-H)2(pyridine)

: 1159404-40-6
EtCo((bis(thiophenyl)glyoxime-H)2(pyridine)

Guidance literature:: With NaOH; sodium borohydride; In ethanol; soln. of Co compd. in EtOH purged with N2 for 10 min, cooled to 0°C under stirring, aq. solns. of NaOH and NaBH4 added, soln. of EtBr in EtOH added, mixt. stirred at 0°C for 1 h, concd. under vac., poured into H20 contg. drops of pyridine; ppt. filtered off, washed with H2O and dried, column chromy. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/om900065k

Reference yield:

: 110-86-1
pyridine

: 1313442-71-5
CoEt(pyridine)(dithiophenylglyoxime(-1H))(dimethylglyoxime(-1H))

: 1159404-40-6
CoEt(pyridine)(dithiophenylglyoxime(-1H))2

Guidance literature:: Multi-step reaction with 2 steps

1: air / ethanol

2: NaBH₄ / not given

With air; NaBH₄; In ethanol;
DOI:10.1016/j.jorganchem.2011.02.033