7-azetidino>-6-p-anisylbenzooctem

Base Information

• Chemical Name: 7-azetidino>-6-p-anisylbenzo
• Molecular Formula: C₃₄H₂₈N₂O₆
• Molecular Weight: 560.606

Synonyms:

Chemical Property of 7-azetidino>-6-p-anisylbenzo

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

There total 9 articles about 7-azetidino>-6-p-anisylbenzooctem which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-(4'-methoxylphenyl)-3,4-dihydroisoquinoline (59224-73-6) + (2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-acetic acid (76640-35-2) → 1-(2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-9b-(4-methoxy-phenyl)-1,4,5,9b-tetrahydro-azeto[2,1-a]isoquinolin-2-one (82934-72-3,87758-71-2)

Guidance literature:

With triethylamine; trichlorophosphate; In dichloromethane; 1) 4h, r.t. 2) 2h, reflux;

Reference yield: 60.0%

(1R,9bR)-1-{[1-Benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-amino}-9b-(4-methoxy-phenyl)-1,4,5,9b-tetrahydro-azeto[2,1-a]isoquinolin-2-one (87702-92-9) + Phenoxyacetyl chloride (701-99-5) → 7-azetidino>-6-p-anisylbenzooctem (82934-72-3,87758-71-2)

Guidance literature:

With triethylamine;

Reference yield:

piperonal (120-57-0,30024-74-9) → 1-(2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-9b-(4-methoxy-phenyl)-1,4,5,9b-tetrahydro-azeto[2,1-a]isoquinolin-2-one (82934-72-3,87758-71-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 70 percent

2: 85 percent / triethylamine / CH₂Cl₂ / 5 h / Ambient temperature

3: 50 percent / aq.NaOH / acetone / 1 h / Heating

4: 70 percent / triethylamine, POCl₃ / CH₂Cl₂ / 1) 4h, r.t. 2) 2h, reflux

With sodium hydroxide; triethylamine; trichlorophosphate; In dichloromethane; acetone;

upstream raw materials:

1-(4'-methoxylphenyl)-3,4-dihydroisoquinoline

(2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-acetic acid

piperonal

{[1-Benzo[1,3]dioxol-5-yl-meth-(Z)-ylidene]-amino}-acetic acid ethyl ester

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