N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

Base Information

Chemical Name:N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide
CAS No.:91421-20-4
Molecular Formula:C₂₄H₂₀N₂O₃
Molecular Weight:384.434
Hs Code.:

N-(1-benzoyl-1,2,2a,3-tetrahydrobenz<cd>indol-4-yl)-N-methylfuran-3-carboxamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

Chemical Property:

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Technology Process of N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

There total 1 articles about N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26214-65-3
furan-3-carbonyl chloride

: 51867-06-2
1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-(5H)-one

: 74-89-5
methylamine

: 91421-20-4
N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

Guidance literature:: With triethylamine; Yield given. Multistep reaction; 1.) benzene, reflux, 5 h.; 2.) benzene, reflux, 2 h.;

Reference yield: 22.0%

: 91421-20-4
N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

: 84936-67-4,84986-20-9,98633-52-4
(3aβ,5aβ,6aβ,11bα,11cβ)-8-benzoyl-5,5a,6,6a,7,8,11b,11c-octahydro-5-methylfuro<3,2-c>indolo<4,3-fg>quinolin-4(3aH)-one

: 84936-67-4,84986-20-9,98633-52-4
(3aβ,5aα,6aα,11bα,11cβ)-8-benzoyl-5,5a,6,6a,7,8,11b,11c-octahydro-5-methylfuro<3,2-c>indolo<4,3-fg>quinolin-4(3aH)-one

: 84936-67-4,84986-20-9,98633-52-4
(3aβ,5aβ,6aα,11bα,11cβ)-8-benzoyl-5,5a,6,6a,7,8,11b,11c-octahydro-5-methylfuro<3,2-c>indolo<4,3-fg>quinolin-4(3aH)-one

Guidance literature:: With sodium tetrahydroborate; In methanol; benzene; for 3h; Irradiation;

Reference yield:

: 91421-20-4
N-(1-benzoyl-1,2,2a,3-tetrahydrobenzindol-4-yl)-N-methylfuran-3-carboxamide

: 62592-69-2
methyl (3β)-1-benzoyl-2,3-dihydroisolysergate

Guidance literature:: Multi-step reaction with 4 steps

2: 83 percent / trimethylamine N-oxide dihydrate / osmium tetraoxide / 2-methyl-propan-2-ol; pyridine; H₂O / 1 h / Heating

3: 1.) sodium metaperiodate; 2.) 4.0M chromium trioxide - sulphuric acid / 1.) methanol, water, room temp., 2 h.; 2.) aceton, water, 0 deg C, 1 h.

4: 85percent phosphoric acid, phosphoryl trichloride / pyridine

With chromium(VI) oxide; sodium periodate; trimethylamine-N-oxide; phosphoric acid; sulfuric acid; trichlorophosphate; osmium(VIII) oxide; In pyridine; water; tert-butyl alcohol;