diazene, 1,2-ditricyclo[3.3.1.1~3,7~]dec-1-yl-, 1,2-dioxide

Base Information

• Chemical Name: diazene, 1,2-ditricyclo[3.3.1.1~3,7~]dec-1-yl-, 1,2-dioxide
• CAS No.: 119135-74-9
• Molecular Formula: C₂₀H₃₀N₂O₂
• Molecular Weight: 330.47
• Mol file: 119135-74-9.mol

Synonyms:

Chemical Property of diazene, 1,2-ditricyclo[3.3.1.1~3,7~]dec-1-yl-, 1,2-dioxide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diazene, 1,2-ditricyclo[3.3.1.1~3,7~]dec-1-yl-, 1,2-dioxide

There total 2 articles about diazene, 1,2-ditricyclo[3.3.1.1~3,7~]dec-1-yl-, 1,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-Adamantanamine (768-94-5) → Di-adamantan-1-yl-diazene N,N'-dioxide (119135-74-9)

Guidance literature:

With sodium perborate; N,N,N',N'-tetraacetylethylenediamine; sodium hydrogencarbonate; In water; ethyl acetate; for 2.5h; Ambient temperature;

DOI:10.1016/S0040-4039(01)89003-1

Reference yield:

1-Adamantanamine (768-94-5) → 1-Nitrosoadamantane (22734-10-7) + Di-adamantan-1-yl-diazene N,N'-dioxide (119135-74-9)

Guidance literature:

With sodium percarbonate; N,N,N',N'-tetraacetylethylenediamine; sodium hydrogencarbonate; In dichloromethane; water; for 3h; Yield given. Title compound not separated from byproducts; Ambient temperature;

upstream raw materials:

1-Adamantanamine