2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee

Base Information

• Chemical Name: 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee
• CAS No.: 110398-04-4
• Molecular Formula: C₃₃H₄₃BrO₅Si
• Molecular Weight: 627.691
• Mol file: 110398-04-4.mol

Synonyms:

Chemical Property of 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee

There total 1 articles about 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

triethyl-bromo-silane (1112-48-7) + 1,6-anhydro-2,3,4-tri-O-benzyl-β-D-glucopyranose (10548-46-6) → 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee (110398-04-4)

Guidance literature:

at 35 - 40 ℃; for 360h; in the dark;

DOI:10.1016/S0040-4039(01)81005-4

Reference yield:

methanol (67-56-1) + 2,3,4-tri-O-benzyl-6-O-triethylsilyl-α-D-glucopyranosyl bromidee (110398-04-4) → methyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In chloroform;

DOI:10.1016/S0040-4039(01)81005-4

upstream raw materials:

triethyl-bromo-silane

1,6-anhydro-2,3,4-tri-O-benzyl-β-D-glucopyranose

Refernces