[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

Base Information

Chemical Name:[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2
CAS No.:1256768-12-3
Molecular Formula:C₃₈H₄₀I₄N₄Pd₂
Molecular Weight:1273.22
Hs Code.:

[PdI<sub>2</sub>(CC(C<sub>6</sub>H<sub>5</sub>)N(CH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>)N(CH(CH<sub>3</sub>)2))]2

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Suppliers and Price of [PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

Chemical Property:

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Technology Process of [PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

There total 1 articles about [PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.9%

: 700816-99-5
1-isopropyl-3-methyl-2,4-diphenylimidazolium iodide

: 3375-31-3
palladium diacetate

: 1256768-12-3
[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

Guidance literature:: In 1,4-dioxane; (Ar); mixt. of Pd salt (0.5 equiv.) and imidazolium salt in dioxane was heated at 80°C for 7 h; cooled to room temp.; evapd.; chromd. (silica gel, CH2Cl2); recrystd. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1021/om100746r

Reference yield: 100.0%

: 626-60-8
3-Chloropyridine

: 1256768-12-3
[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

: 1256768-15-6
[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))(NC₅H₄Cl)]

Guidance literature:: In dichloromethane; (Ar); chloropyridine was added to Pd complex in CH2Cl2; stirred at room temp. for 2 h; evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om100746r

Reference yield: 65.8%

: 75-09-2
dichloromethane

: 700816-99-5
1-isopropyl-3-methyl-2,4-diphenylimidazolium iodide

: 1256768-12-3
[PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))]2

: [PdI₂(CC(C₆H₅)N(CH₃)C(C₆H₅)N(CH(CH₃)2))2]*CH₂Cl₂

Guidance literature:: With Ag₂O; In dichloromethane; (Ar); Ag2O and imidazolium salt were mixed with CH2Cl2; stirred at room temp. for 4 h; filtered through Celite; mixed with Pd complex; stirred at room temp. for 5 h; chromd. (silica gel, CH2Cl2); recrystd. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1021/om100746r