3-(4-BROMOPHENYL)-4'-METHOXYPROPIOPHENONE

Base Information

• Chemical Name: 3-(4-BROMOPHENYL)-4'-METHOXYPROPIOPHENONE
• CAS No.: 150405-65-5
• Molecular Formula: C₁₆H₁₅BrO₂
• Molecular Weight: 319.198
• Mol file: 150405-65-5.mol

Synonyms:

Chemical Property of 3-(4-BROMOPHENYL)-4'-METHOXYPROPIOPHENONE

Chemical Property:

Purity/Quality:

3-(4-bromophenyl)-4'-methyoxypropiophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-(4-BROMOPHENYL)-4'-METHOXYPROPIOPHENONE

There total 7 articles about 3-(4-BROMOPHENYL)-4'-METHOXYPROPIOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-bromo-4'-methoxychalcone (92873-00-2) → 3-(4-bromophenyl)-1-(4-methoxyphenyl)propan-1-one (150405-65-5)

Guidance literature:

With methanol; C₂₅H₂₉ClNO₂Rh; potassium carbonate; at 90 ℃; for 1h; chemoselective reaction;

DOI:10.1016/S1872-2067(19)63367-X

Reference yield: 86.0%

4-bromobenzenemethanol (873-75-6) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 3-(4-bromophenyl)-1-(4-methoxyphenyl)propan-1-one (150405-65-5)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; triphenylphosphine; potassium hydroxide; at 100 ℃; for 6h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201410391

Reference yield: 85.0%

1-(4-methoxyphenyl)cyclopropan-1-ol (15973-65-6) + 4-Bromophenylboronic acid (5467-74-3) → 3-(4-bromophenyl)-1-(4-methoxyphenyl)propan-1-one (150405-65-5)

Guidance literature:

With copper diacetate; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; In water; dimethyl sulfoxide; at 70 ℃; for 2h; chemoselective reaction;

DOI:10.1021/acs.joc.0c00160

upstream raw materials:

1-(4-methoxylphenyl)-2-propen-1-ol

4-Bromophenylboronic acid

4-bromobenzenemethanol

1-(4-methoxyphenyl)ethanone

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